Several techniques are employed for effective synthesis monitoring:
Spectroscopy: Techniques like UV-Vis, IR, and Raman spectroscopy are used to analyze the chemical composition and structure of nanomaterials. Microscopy: Electron microscopy (TEM and SEM) and atomic force microscopy (AFM) provide high-resolution images to study the morphology and size of nanomaterials. X-ray Diffraction (XRD): This technique is used to determine the crystalline structure of nanomaterials. Dynamic Light Scattering (DLS): DLS helps in measuring the size distribution of nanoparticles in a solution. Thermogravimetric Analysis (TGA): TGA is used to assess the thermal stability and composition of nanomaterials.